Antioxidant BHT 264
CAS:128-37-0
Purity:99%
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Product Details
Three ionic liquids with borate anions o...
The invention belongs to the technical f...
The invention discloses a preparation me...
The invention relates to the technical f...
The invention provides a preparation met...
boron trifluoride
lithium oxalate
lithium difluoromono[1,2-oxalato(2-)-O,O'] borate
| Conditions | Yield |
|---|---|
|
With
hydrogen fluoride;
at 30 ℃;
for 4h;
Temperature;
|
98.23% |
|
boron trifluoride; lithium oxalate;
With
carbonic acid dimethyl ester;
In
diethyl ether;
at 75 ℃;
for 8h;
Inert atmosphere;
With
boron trifluoride; potassium oxalate; carbonic acid dimethyl ester;
In
diethyl ether;
at 80 ℃;
for 28h;
Solvent;
Temperature;
Reagent/catalyst;
Inert atmosphere;
|
94.1% |
|
lithium oxalate;
With
hydrogen fluoride;
at 20 ℃;
for 6h;
Sealed tube;
Large scale;
boron trifluoride;
at 20 ℃;
Sealed tube;
Large scale;
|
91.5% |
boron trifluoride dimethyl carbonate complex
oxalic acid
lithium chloride
lithium difluoromono[1,2-oxalato(2-)-O,O'] borate
| Conditions | Yield |
|---|---|
|
oxalic acid; lithium chloride;
With
carbonic acid dimethyl ester;
In
water;
at 80 ℃;
for 1h;
under 760.051 Torr;
Inert atmosphere;
boron trifluoride dimethyl carbonate complex;
In
water;
for 1.5h;
Inert atmosphere;
|
91% |
oxalic acid
ethanedioic acid bis(trimethylsilyl)ester
lithium hexafluorophosphate
boron trifluoride diethyl etherate
lithium bis[1,2-oxalato(2-)-O,O'] borate
