Antioxidant BHT 264
CAS:128-37-0
Purity:99%
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Product Details
Synthesis Reference(s) |
Organic Syntheses, Coll. Vol. 2, p. 425, 1943Tetrahedron Letters, 22, p. 1013, 1981 DOI: 10.1016/S0040-4039(01)82853-7 |
Purification Methods |
Crystallise the acid from toluene (3mL/g) (charcoal), pet ether (b 80-100o), or aqueous 50% EtOH. The amide has m 202o (from EtOH). [Beilstein 9 IV 2402.] |
InChI:InChI=1/C11H8O2/c12-11(13)10-7-3-5-8-4-1-2-6-9(8)10/h1-7H,(H,12,13)/p-1
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p-nitrophenyl 1-naphthoate
4-nitro-phenol
1-naphthalenecarboxylic acid
Conditions | Yield |
---|---|
With
erythromycin A-hydrolyse prod.; water;
In
1,4-dioxane;
at 20 ℃;
Rate constant;
pH 12.052;
|
1-(4-methoxyphenyl)-2-(naphthalen-1-yl)ethan-1-one
1-naphthalenecarboxylic acid
4-methoxybenzoic acid
Conditions | Yield |
---|---|
With
oxygen; potassium hydroxide;
at 20 ℃;
chemoselective reaction;
Schlenk technique;
|
92% 92% |
1'-naphthacetophenone
n-butyllithium
naphthalene
diethyl ether
2-naphthalen-1-yl-4,5-dihydro-1H-imidazole
tetralin-1-carboxylic acid
5,6,7,8-tetrahydro-1-naphthalenecarboxylic acid
decalin-1-carboxylic acid